Browsing by Subject "dispersion"
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Item A study of micro fiber dispersion using digital image analysis(Texas A&M University, 2004-11-15) Hendrarsakti, JoonedThe area of the digital image processing is getting more attention in the hope that it will increase the accuracy of any scientific measurements, such as in determining an object velocity, temperature, and size. While human vision is excellent to recognize and differentiate objects, it has been proven to be a poor tool when it comes to measure the object performance. One of many digital image processing applications is texture analysis whose purpose is to evaluate image patterns. The purpose of this dissertation is to investigate the use of texture analysis as a tool to micro fiber dispersion measurement. Micro fiber dispersion can be found in many applications such as in paper and industry powder engineering. Three cases related to micro fiber dispersion were investigated in this study. The first case was the experimental study of the dispersion in open water channel. Sets of synthetic fibers were put into water channel to simulate a process that can be found in papermaking industry. The research investigated the effect of three operating parameters: fluid velocity, fiber consistency, and fiber aspect ratio to fiber dispersion. Using two-factorial experimental design technique, the main and interaction effects of these parameters were evaluated. The study found that increasing fluid velocity, fiber aspect ratio, and consistency decreased the dispersion level. The study also found that the effect of individual parameters is more pronounced than the role of the interactive terms on the fiber flocculation. The second case considered was applying the fiber dispersion analysis to computer-synthesized images consisting of different arrangements of fibers. Four sets of sub-cases were presented. These sub-cases were divided based on the fiber-concentrated location and fiber distribution. The use of computer-synthesized images was found to be very useful to simulate real situation during fiber dispersion. The third case investigated the fiber distribution on a dry paper. Images for different types of paper were taken and evaluated to see the dispersion level of each type of paper. It was found that the current texture analysis was applicable to determine the dispersion level for dry papers. While three cases indicated that the texture analysis can be used to investigate the fiber dispersion, the texture analysis used here is not a perfect and universal method and may not be suitable to analyze other types of dispersions. The human vision will always be essential to determine if the texture analysis is applicable to any other problem.Item Beam-Scanning Reflectarray Enabled by Fluidic Networks(2012-02-14) Long, StephenThis work presents the design, theory, and measurement of a phase-reconfigurable reflectarray (RA) element for beamforming applications enabled by fluidic networks and colloidal dispersions. The element is a linearly polarized microstrip patch antenna loaded with a Coaxial Stub Microfluidic Impedance Transformer (COSMIX). Specifically, adjusting the concentration of highly dielectric particulate in the dispersion provides localized permittivity manipulation within the COSMIX. This results in variable impedance load on the patch and ultimately continuous, low-loss phase control of a signal reflected from the patch. Different aspects of design, modeling, and measurement are discussed for a proof-of-concept prototype and three further iterations. Initial measurements with manual injections of materials into a fabricated proof-of-concept demonstrate up to 200 degrees of phase shift and a return loss of less than 1.2 dB at the operating frequency of 3 GHz. The next design iteration addresses fabrication challenges as well the general cumbersomeness of the proof-of-concept by replacing the static material delivery system with a dynamic closed-loop fluidic network. It also makes use of a design procedure to maximize the phase sensitivity. Measurements demonstrate progressive phase shifts through dilution of the system reservoir; however, the initial measurements with this system are not in line with simulated predictions. Investigations suggest the primary culprit to be inaccurate material data. The dielectric constant of the particulate (colloidal BSTO) was overrated and the loss tangent of the fluid medium (a silicone-based oil) was underrated. After accounting for these issues the measurement a second measurement with the system demonstrates 270 degrees of phase shift with return loss of 9 dB. The next design iteration examines a trade-off between phase sensitivity and reduced losses. The design also features modifications to the fluidic system to allow for layered fabrication in the GND plane as well integration with a 2-port coaxial measurement cell. Attempted measurements discover the fluidic system cannot flow the higher concentrations of nanoparticles necessary for phase shifting. A final design iteration addresses this challenge by expanding and repositioning inlets to the fluidic system. Free space reflection measurements with this element initially demonstrate phase shifting until a buildup of nanoparticles form within the COSMIX.Item Carbon nanotube and nanofiber reinforcement for improving the flexural strength and fracture toughness of portland cement paste(2012-07-16) Tyson, Bryan MichaelThe focus of the proposed research will be on exploring the use of nanotechnology-based nano-filaments, such as carbon nanotubes (CNTs) and nanofibers (CNFs), as reinforcement in improving the mechanical properties of portland cement paste as a construction material. Due to their ultra-high strength and very high aspect ratios, CNTs and CNFs have been used as excellent reinforcements in enhancing the physical and mechanical properties of polymer, metallic, and ceramic composites. Very little attention has been devoted on exploring the use of nano-filaments in the transportation industry. Therefore, this study aims to bridge the gap between nano-filaments and transportation materials. This will be achieved by testing the integration of CNTs and CNFs in ordinary portland cement paste through state-of-the-art techniques. Different mixes in fixed proportions (e.g. water-to-cement ratio, air content, admixtures) along with varying concentrations of CNTs or CNFs will be prepared. Different techniques commonly used for other materials (like polymers) will be used in achieving uniform dispersion of nano-filaments in the cement paste matrix and strong nano-filaments/cement bonding. Small-scale specimens will be prepared for mechanical testing in order to measure the modified mechanical properties as a function of nano-filaments concentration, type, and distribution. With 0.1 percent CNFs, the ultimate strain capacity increased by 142 percent, the flexural strength increased by 79 percent, and the fracture toughness increased by 242 percent. Furthermore, a scanning electron microscope (SEM) is used to discern the difference between crack bridging and fiber pullout. Test results show that the strength, ductility, and fracture toughness can be improved with the addition of low concentrations of either CNTs or CNFs.Item Dispersion in analysts' forecasts: does it make a difference?(Texas A&M University, 2004-09-30) Adut, DavitFinancial analysts are an important group of information intermediaries in the capital markets. Their reports, including both earnings forecasts and stock recommendations, are widely transmitted and have a significant impact on stock prices (Womack 1996; Lys and Sohn 1990, among others). Empirical accounting research frequently relies on analysts' forecasts to construct proxies for variables of interest. For example, the error in mean forecast is used as a proxy for earnings surprise (e.g., Brown et al.1987; Wiedman 1996; Bamber et al.1997). More recent papers provide evidence that the mean consensus forecast is used as a benchmark for evaluating firm performance. (Degeorge et al. 1999; Kasznik and McNichols 2002; Lopez and Rees 2002). Another stream of research uses the forecast dispersion as a proxy for the uncertainty or the degree of consensus among analysts and focuses on the information properties of analysts (e.g., Daley et al. 1988; Ziebart 1990; Imhoff and Lobo 1992; Lang and Lundholm 1996; Barron and Stuerke 1998; Barron et al. 1998). In this paper I combine the two streams of research, and investigate how lack of consensus changes the information environment of analysts and whether the markets perceive this change. More specifically, I investigate the amount of private information in a divergent earnings estimate (i.e. one that is above or below the consensus), whether the markets react to it at either the time of the forecast release, at the realization of actual earnings, and whether Regulation Fair Disclosure has changed the information environment differently for high and low dispersion firms.Item Fast amplitude and delay measurement for characterization of optical devices(Texas A&M University, 2006-10-30) Thompson, Michael ThomasA fast measurement technique based on the modulation phase-shift technique is developed to measure the wavelength-dependent magnitude and phase responses of optical devices. The measured phase response is in the form of group delay, which is used to determine the chromatic dispersion in the device under test by taking the derivative of the group delay with respect to optical wavelength. The measurement setup allows both step-tunable and sweeping laser sources. A modulation frequency of up to 2.7 GHz is accommodated. An alternate method for the phase measurement that overcomes non-linearities in the measurement setup is also presented. The speed of the measurement setup is limited by the sweeping speed of the laser source, which for the Agilent 81682A is 40 nm/sec. The magnitude accuracy is determined by taking a comparison to the commercially available Micron Finisar measurement system, where an error of 0.125 dB is noted. The phase accuracy of the measurement setup is tested by taking the Hilbert transform of the measured magnitude response of an Acetylene gas cell and comparing it to the integral of the measured group delay. The average deviation between the two methods is 0.1 radians. An Acetylene gas cell, fiber Bragg grating, and chirped Bragg grating are tested with the measurement setup and the Agilent 8168The characterization of the setup leads to the conclusion that the measurement setup developed in this paper is fast and accurate. The speed of the technique is on the order of microseconds for a single measurement and excels beyond the speed of the standard modulation phase-shift technique, which includes measurement times on the order of minutes. The accuracy of the technique is within 0.125 dB for magnitude measurements and 0.1 radians for phase measurements when compared to commercially available measurement systems.2A laser source at 40 nm/sec and the measurement plots are presented.Item Forced Dispersion of Liquefied Natural Gas Vapor Clouds with Water Spray Curtain Application(2011-02-22) Rana, Morshed A.There has been, and will continue to be, tremendous growth in the use and distribution of liquefied natural gas (LNG). As LNG poses the hazard of flammable vapor cloud formation from a release, which may result in a massive fire, increased public concerns have been expressed regarding the safety of this fuel. In addition, regulatory authorities in the U.S. as well as all over the world expect the implementation of consequence mitigation measures for LNG spills. For the effective and safer use any safety measure to prevent and mitigate an accidental release of LNG, it is critical to understand thoroughly the action mechanisms. Water spray curtains are generally used by petro-chemical industries to prevent and mitigate heavier-than-air toxic or flammable vapors. It is also used to cool and protect equipment from heat radiation of fuel fires. Currently, water spray curtains are recognized as one of the economic and promising techniques to enhance the dispersion of the LNG vapor cloud formed from a spill. Usually, water curtains are considered to absorb, dilute, disperse and warm a heavier-than-air vapor cloud. Dispersion of cryogenic LNG vapor behaves differently from other dense gases because of low molecular weight and extremely low temperature. So the interaction between water curtain and LNG vapor is different than other heavier vapor clouds. Only two major experimental investigations with water curtains in dispersing LNG vapor clouds were undertaken during the 1970s and 1980s. Studies showed that water spray curtains enhanced LNG vapor dispersion from small spills. However, the dominant phenomena to apply the water curtain most effectively in controlling LNG vapor were not clearly demonstrated. The main objective of this research is to investigate the effectiveness of water spray curtains in controlling the LNG vapor clouds from outdoor experiments. A research methodology has been developed to study the dispersion phenomena of LNG vapor by the action of different water curtains experimentally. This dissertation details the research and experiment development. Small scale outdoor LNG spill experiments have been performed at the Brayton Fire Training Field at Texas A&M University. Field test results regarding important phenomena are presented and discussed. Results have determined that the water curtains are able to reduce the concentration of the LNG vapor cloud, push the vapor cloud upward and transfer heat to the cloud. These are being identified due to the water curtain mechanisms of entrainment of air, dilution of vapor with entrained air, transfer of momentum and heat to the gas cloud. Some of the dominant actions required to control and disperse LNG vapor cloud are also identified from the experimental tests. The gaps are presented as the future work and recommendation on how to improve the experiments in the future. This will benefit LNG industries to enhance its safety system and to make LNG facilities safer.Item Production, Characterization, and Mechanical Behavior of Cementitious Materials Incorporating Carbon Nanofibers(2012-10-19) Yazdanbakhsh, ArdavanCarbon nanotubes (CNTs) and carbon nanofirbers (CNFs) have excellent properties (mechanical, electrical, magnetic, etc.), which can make them effective nanoreinforcements for improving the properties of materials. The incorporation of CNT/Fs in a wide variety of materials has been researched extensively in the past decade. However, the past study on the reinforcement of cementitious materials with these nanofilaments has been limited. The findings from those studies indicate that CNT/Fs did not significantly improve the mechanical properties of cementitious materials. Two major parameters influence the effectiveness of any discrete inclusion in composite material: The dispersion quality of the inclusions and the interfacial bond between the inclusions and matrix. The main focus of this dissertation is on the dispersion factor, and consists of three main tasks: First a novel thermodynamic-based method for dispersion quantification was developed. Second, a new method, incorporating the utilization of silica fume, was devised to improve and stabilize the dispersion of CNFs in cement paste. And third, the dispersion quantification method and mechanical testing were employed to measure, compare, and correlate the dispersion and mechanical properties of CNF-incorporated cement paste produced with the conventional and new methods. Finally, the main benefits, including the increase in strength and resistance to shrinkage cracking, obtained from the utilization of CNFs in cement paste will be presented. The investigations and the corresponding results show that the novel dispersion quantification method can be implemented easily to perform a wide variety of tasks ranging from measuring dispersion of nanofilaments in composites using their optical/SEM micrographs as input, to measuring the effect of cement particle/clump size on the dispersion of nano inclusions in cement paste. It was found that cement particles do not affect the dispersion of nano inclusions in cement paste significantly while the dispersion of nano inclusions can notably degenerates if the cement particles are agglomerated. The novel dispersion quantification method shows that, the dispersion of CNFs in cement paste significantly improves by utilizing silica fume. However, it was found that the dispersion of silica fume particles is an important parameter and poorly dispersed silica fume cannot enhance the overall dispersion of nano inclusions in cementitious materials. Finally, the mechanical testing and experimentations showed that CNFs, in absence of moist curing, even if poorly dispersed, can provide important benefits in terms of strength and crack resistance.